Characterization of Active Carbon Prepared from Coconuts Shells using FTIR, XRD and SEM Techniques

Andi Ikhtiar Bakti, Paulus Lobo Gareso

Abstract


Activated carbon is produced from coconut shells through physical and chemical activation. With pyrolysis method, the optimum activation temperature for physics activation is 600oC, and for chemical, activation is to soak it in activator ZnCl2 10% and Na2Ca3 10%. Activated carbon was analyzed by Fourier Transformation Infrared (FTIR) and X-ray Diffraction (XRD) methods. The FTIR result showed that the coconut shells succeeds in becoming carbon. The XRD results confirm the existence of several phases of crystals like graphite around the peaks of 36o and 44o, there are two wide diffraction peaks and can be interconnected with carbon and graphite content. The SEM result showed that the carbonization of pyrolysis and activation processes created porosity and a large surface area for absorption.

Keywords: activated carbon, coconut shell, FTIR, SEM, XRD


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References


A.R Hidayu, N. M. (2016). Preparation and characterization of impregnated activated carbon from palm kernel shell coconut shell for CO2 capture. Procedia Engineering 148, 106–113.

Arami-Niya, A., Daud, W. M. A. W., Mjalli, F. S., Abnisa, F., & Shafeeyan, M. S. (2012). Production of microporous palm shell based activated carbon for methane adsorption: modeling and optimization using response surface methodology. Chemical Engineering Research and Design, 776–784.

Cocommunity, T. (2016). Initiatives Towards Product Diversification Seek Out Viable Opportunities in the Coconut Industry. Monthly Newsletter of the Asian and Pacific Coconut Community, XLVI(8), 1–32.

Fan, M., Dai, D., & Huang, B. (2012). Fourier Transform Infrared Spectroscopy for Natural Fibers. Retrieved from www.intechopen.com

Hesas, R. H., Arami-Niya, A., Daud, W. M. A. W., & Sahu, J. N. (2013). Preparation and Characterization of Activated Carbon from Apple Waste by Microwave-Assisted Phosphoric Acid Activation: Application in Methylene Blue Adsorption. Bio Resources, 8(2), 2950–2966.

Hidayu, A. ., Muhammad, N. F., Matali, S., & Sharifah, A. S. . (2013). Characterization of activated carbon prepared from oil palm empty fruit bunch using BET and FTIR techniques. Procedia Engineering 68, 379–384.

Hung, J. J. (2012). The Production of Activated carbon from Coconut Shells Using Pyrolysis and Fluidized Bed Reactors. Arizona: The University of Arizona.

Kushwaha, S., Padmaja, P., & Sreelatha, G. (2012). Physical and Chemical Modified Forms of Palm Shell Preparation, Characterization, and Preliminary Assessment. Retrieved from https://www.research.net/publication/257594337, 1-17

Lehmann, J., & Joseph, S. (2009). Biocha for environmental management. Earthscan.

Matali, S., Khairuddin, S. A., Sharifah, A. S. A. K., & Hidayu, A. R. (2013). Removal of Selected Gaseous Effluent Using Activated Carbon Derived from Oil Palm Waste: An Overview. IEEE Symposium on Business, Engineering, and Industrial Applications.

NB, O., N, S., & Y, U. (2016). The activated carbon of Oil Palm Empty Fruit (EFB); Core and Shaggy. Procedia Engineering 148, 758–764.

Pradhan, S. (2011). Production and characterization of Activated Carbon produced a suitable Industrial sludge. Odisha, India: Department of Chemical Engineering National Institute of Technology Rourkela.

Promdee, K., Chanvidhwatanakit, J., Satitkune, S., Boonmee, C., Kawichai, T., Jarernprasert, S., & Vitidsant, T. (2017). Characterization of Carbon Materials and Differences from Activated Carbon Particle (ACP) and Coal Briquettes Product (CBP) Derived From Coconut Shell Via Rotary Kiln. Renewable and Sustainable Energy Reviews 75, 1175–1186.

Rani, N. H. A., Mohammad, nor F., Matali, S., & Kadir, S. A. S. A. (2014). Preparation and characterization of activated carbon made from oil palm empty fruit bunch. Engineering Materials, 594–595.

Rao, K. V., A.H.L.Swaroop, Rao, D. P. K. R., & Bharath, C. N. (2015). Study on Strength Properties of Coconut Shell Concrete. International Journal of Civil Engineering and Technology (IJCIET), 42–61.




DOI: http://dx.doi.org/10.24042/jipfalbiruni.v7i1.2459

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Jurnal Ilmiah Pendidikan Fisika Al-Biruni is licensed under a Creative Commons Attribution-ShareAlike 4.0 International License. Copyright © UIN Raden Intan Lampung. All rights reservedp-ISSN 2303-1832 | e-ISSN 2503-023X